16a,30-DIHIDROXI-FRIEDELAN-3-ONA(CELASDINA A)
16a,30-DIHIDROXI-FRIEDELAN-3-ONA
(CELASDINA A)
RMN de 1H |
Atrib |
d |
Mult |
J |
Atrib |
d |
Mult |
J |
1 |
1,68; 1,67 |
m (2H) |
19 |
1,50 |
m (2H) |
|||
2 |
2,35 |
m (2H) |
21 |
1,17; 1,45 |
m (2H) |
|||
4 |
2,22 |
m (1H) |
22 |
1,28; 1,33 |
m (2H) |
|||
6 |
1,26; 1,75 |
m (2H) |
23 |
0,85 |
d (3H) |
6,8 |
||
7 |
1,32; 1,47 |
m (2H) |
24 |
0,69 |
s (3H) |
|||
8 |
1,38 |
m (1H) |
25 |
0,83 |
s (3H) |
|||
10 |
1,50 |
m (1H) |
26 |
1,03 |
s (3H) |
|||
11 |
1,21; 1,40 |
m (2H) |
27 |
0,98 |
s (3H) |
|||
12 |
1,32 |
m (2H) |
28 |
1,12 |
s (3H) |
|||
15 |
1,26; 1,78 |
m (2H) |
29 |
0,97 |
s (3H) |
|||
16 |
4,0 |
t (1H) |
8,9 |
30 |
3,46; 3,36 |
q (2H) |
10,6 |
|
18 |
1,52 |
m (1H) |
| RMN de 13C | C |
d |
C |
d |
C |
d |
1 |
22,20 |
11 |
35,60 |
21 |
29,63 | |
2 |
41,40 |
12 |
30,70 |
22 |
35,00 | |
3 |
213,0 |
13 |
40,10 |
23 |
6,80 | |
4 |
58,10 |
14 |
39,10 |
24 |
14,60 | |
5 |
42,20 |
15 |
44,10 |
25 |
18,10 | |
6 |
41,10 |
16 |
75,30 |
26 |
19,90 | |
7 |
18,40 |
17 |
35,60 |
27 |
21,30 | |
8 |
53,30 |
18 |
44,50 |
28 |
25,09 | |
9 |
37,40 |
19 |
27,54 |
29 |
29,30 | |
10 |
59,40 |
20 |
33,30 |
30 |
70,60 |
Phytochemistry, 44(7), 1275-1281, 1997
