6b-HIDROXI-LUPAN-20(30)-EN-3-ONA
6b-HIDROXI-LUPAN-20(30)-EN-3-ONA
RMN de 1H (CDCl3)
|
Atrib |
d |
Mult |
J |
Atrib |
d |
Mult |
J |
0,81 |
s (3H) |
22 |
1,96 |
m (2H) |
||||
0,91 |
s (3H) |
2a |
2,26 |
ddd (1H) |
15,01; 6,48; 2,85 | |||
1,14 |
s (3H) |
19 |
2,40 |
ddd (1H) |
11,07; 5,35; 5,59 | |||
1,41 |
s (3H) |
2b |
2,82 |
ddd (1H) |
15,01; 6,41; 2,91 | |||
1,42 |
s (3H) |
6 |
4,48 |
s br (1H) |
||||
1,43 |
s (3H) |
30 |
4,58 |
d br (1H) |
2,50 | |||
1,68 |
s (3H) |
30 |
4,68 |
d br (1H) |
2,47 | |||
1,73 |
m (2H) |
| RMN de 13C (CDCl3) | C |
d |
C |
d |
C |
d |
1 |
42,29 |
11 |
21,34 |
21 |
29,89 |
|
2 |
34,58 |
12 |
25,25 |
22 |
40,05 |
|
3 |
217,39 |
13 |
37,25 |
23 |
25,06 |
|
4 |
49,11 |
14 |
42,24 |
24 |
23,80 |
|
5 |
56,75 |
15 |
27,58 |
25 |
17,02 |
|
6 |
69,90 |
16 |
35,28 |
26 |
17,14 |
|
7 |
42,29 |
17 |
43,24 |
27 |
14,85 |
|
8 |
40,15 |
18 |
48,48 |
28 |
18,05 |
|
9 |
50,84 |
19 |
48,09 |
29 |
109,77 |
|
10 |
36,87 |
20 |
151,25 |
30 |
19,38 |
Phytochemistry, 30(10), 3490-3493, 1991
