NETZASCUTIONINA
Aa
RMN de 1H (CDCl3) 400MHz |
Atrib |
d |
Mult |
J |
Atrib |
d |
Mult |
J |
0,80 | s (3H) | 1 |
6,03 |
d |
1,4 |
|||
0,87 |
s (3H) |
6 |
6,54 |
dd |
1,4; 6,4 | |||
1,01 |
s (3H) |
7 |
5,75 |
d |
6,4 | |||
1,07 |
s (3H) |
23 |
1,56 |
s |
||||
1,12 |
s (3H) |
1' |
6,71 |
s |
||||
1,15 |
s (3H) |
6' |
6,64 |
dd |
2,8; 10,0 |
|||
1,18 |
s (3H) |
7' |
5,91 |
dd |
2,6; 10,0 |
|||
1,20 |
s (6H) |
23' |
2,08 |
s |
||||
1,70 |
s (3H) |
OMe |
3,67 |
s |
||||
OH |
4,93 |
s (1H) |
OMe |
3,68 |
s |
RMN de 13C
|
C |
d (mult) |
C |
d (mult) |
C |
d (mult) |
C |
d (mult) |
1 |
115,37d |
6' |
124,02d |
29,99t |
36,50t |
|||
2 |
190,55s |
7' |
129,19d |
29,99t |
37,96t |
|||
3 |
91,39s |
8' |
45,53d |
30,39s |
38,98s |
|||
4 |
78,36s |
9' |
37,50s |
30,65t |
39,03s |
|||
5 |
131,53s |
10' |
143,68s |
31,20t |
40,59s |
|||
6 |
127,56d |
10,92q |
31,57q |
42,11s |
||||
7 |
120,29d |
16,97q |
31,79q |
42,66s |
||||
8 |
151,03s |
17,49q |
32,20q |
44,04d |
||||
9 |
44,14s |
19,79q |
33,67s |
44,45d |
||||
10 |
170,18s |
22,17q |
33,97t |
OMe |
51,59q |
|||
1' |
108,15d |
22,27q |
35,61t |
OMe |
51,84q |
|||
2' |
140,07s |
23,00q |
35,96t |
128,56s |
||||
3' |
137,79s |
27,23q |
36,11t |
134,66s |
||||
4' |
122,54s |
28,44q |
36,25t |
179,34s |
||||
5' |
125,07s |
28,67t |
36,44t |
179,34s |
Tetrahedron, 52(28), 9597-9608, 1996