7,8-DIHIDRO-ESCUTIDINA
Ba
RMN de 1H (CDCl3) 400MHz |
Atrib |
d |
Mult |
J |
Atrib |
d |
Mult |
J |
0,62 |
s (3H) |
OH |
4,93 |
s br |
||||
0,76 |
s (3H) |
1 |
5,98 |
s |
||||
0,99 |
s (3H) |
6 |
6,33 |
s br |
||||
1,06 |
s (3H) |
7 |
2,14 |
m |
||||
1,08 |
s (3H) |
23 |
1,48 |
s |
||||
1,11 |
s (3H) |
1' |
6,97 |
s |
||||
1,18 |
s (3H) |
7' |
6,23 |
s |
||||
1,19 |
s (3H) |
23' |
2,53 |
s |
||||
1,30 |
s (3H) |
OMe |
3,55 |
s |
||||
1,54 |
s (3H) |
OMe |
3,65 |
s |
RMN de 13C
|
C |
d (mult) |
C |
d (mult) |
C |
d (mult) |
C |
d (mult) |
1 |
112,70d |
6' |
186,85s |
29,41s |
35,70t |
|||
2 |
191,20s |
7' |
125,95d |
29,52t |
36,07t |
|||
3 |
90,95s |
8' |
170,58s |
29,59t |
37,08s |
|||
4 |
79,15s |
9' |
39,75s |
29,87s |
37,33q |
|||
5 |
133,72s |
10' |
151,41s |
30,19t |
38,56s |
|||
6 |
133,72s |
13,01q |
30,19t |
38,68q |
||||
7 |
29,09t |
15,69q |
30,31t |
40,18s |
||||
8 |
41,29d |
16,53q |
30,68t |
40,25s |
||||
9 |
39,81s |
18,23q |
31,29q |
43,94d |
||||
10 |
169,81s |
20,53q |
31,35q |
44,31d |
||||
1' |
110,14d |
21,77t |
32,97q |
44,36s |
||||
2' |
144,17s |
22,40q |
32,58q |
OMe |
51,23q |
|||
3' |
137,94s |
23,84t |
33,88t |
OMe |
51,23q |
|||
4' |
129,03s |
28,01t |
34,63t |
178,66s |
||||
5' |
122,94s |
28,21t |
35,70t |
178,88s |
Tetrahedron
, 52(28), 9597-9608, 1996