ESCUTIONINA Aa
RMN de 1H (CDCl3) 400MHz |
Atrib |
d |
Mult |
J |
Atrib |
d |
Mult |
J |
0,53 |
s (3H) |
6 |
6,32 |
dd |
6,3; 1,2 |
|||
0,87 |
s (3H) |
7 |
5,92 |
d |
6,3 |
|||
0,99 |
s (3H) |
23 |
1,53 |
s |
||||
1,06 |
s (3H) |
1' |
6,70 |
s |
||||
1,07 |
s (3H) |
6' |
6,63 |
dd |
2,7; 10,2 |
|||
1,11 |
s (3H) |
7' |
5,90 |
dd |
2,5; 10,2 |
|||
1,17 |
s (3H) |
23' |
2,05 |
s |
||||
1,21 |
s (3H) |
OMe |
3,58 |
s |
||||
1,41 |
s (3H) |
OMe |
3,67 |
s |
||||
1 |
6,06 |
d |
1,2 |
RMN de 13C
|
C |
d (mult) |
C |
d (mult) |
C |
d (mult) |
C |
d (mult) |
1 |
115,60d |
6' |
124,01d |
29,70t |
36,01t |
|||
2 |
191,12s |
7' |
129,12d |
29,80t |
36,33t |
|||
3 |
91,81s |
8' |
45,51d |
30,02t |
36,41t |
|||
4 |
78,73s |
9' |
38,23s |
30,41s |
38,93s |
|||
5 |
130,70s |
10' |
143,72s |
30,52t |
39,01s |
|||
6 |
126,34d |
10,91q |
30,60s |
40,41s |
||||
7 |
116,30d |
17,03q |
31,02t |
40,52s |
||||
8 |
160,51s |
17,50q |
31,22t |
44,24d |
||||
9 |
41,62s |
18,31q |
31,5q |
44,32s |
||||
10 |
173,71s |
22,24q |
31,81q |
44,41d |
||||
1' |
108,03d |
22,24q |
32,20q |
44,51s |
||||
2' |
140,04s |
22,50q |
32,84q |
OMe |
51,62q |
|||
3' |
137,61s |
28,21t |
32,91t |
OMe |
51,62q |
|||
4' |
122,42s |
28,32t |
34,81t |
178,91s |
||||
5' |
125,02s |
29,51t |
34,90q |
179,33s |
Tetrahedron
, 52(28), 9597-9608, 1996