FRIEDELAN-3a-OL(3a -FRIEDELINOL)
FRIEDELAN-3a-OL
(3a -FRIEDELINOL)
RMN de 1H 400 MHz (CDCl3/C5D5N) |
Atrib |
d |
Mult |
J |
Atrib |
d |
Mult |
J |
1eq |
1,35 | m (1H) |
18ax |
1,54 | m (1H) |
|||
1ax |
1,58 | m (1H) |
19ax |
1,24 | d (1H) |
6 |
||
2ax |
1,38 | m (1H) |
19eq |
1,41 | m (1H) |
|||
2eq |
2,16 | dq (1H) |
13,0; 3,0 |
21ax |
1,46 | m (1H) |
||
3 |
3,41 | td (1H) |
10,4 |
21eq |
1,25 | m (1H) |
||
4 |
1,17 | m (1H) |
22ax |
1,45 | dd (1H) |
5,0; 2,0 | ||
6ax |
1,19 | m (1H) |
22eq |
0,89 | m (1H) |
|||
6eq |
1,75 | dt (1H) |
1,,0; 2,0 |
23 |
1,01 | d (3H) |
6,0 |
|
7 |
1,32 e 1,38 | m (2H) |
24 |
0,78 | s (3H) |
|||
8 |
1,28 | m(1H) |
25 |
0,81 | s (3H) |
|||
10ax |
1,00 | m (1H) |
26 |
0,98 | s (3H) |
|||
11 |
1,18 e 1,38 | m (2H) |
27 |
1,01 | s (3H) |
|||
12 |
1,26 e 1,31 | m (2H) |
28 |
1,18 | s (3H) |
|||
15ax |
1,52 | m (1H) |
29 |
0,97 | s (3H) |
|||
15eq |
1,28 | m (1H) |
30 |
1,02 | s (3H) |
|||
16 |
1,26 e 1,48 | m (2H) |
| RMN de 13C 100 MHz (CDCl3/C5D5N) | C |
d |
C |
d |
C |
d |
1 |
19,76 | 11 |
35,57 | 21 |
32,88 | |
2 |
37,00 | 12 |
30,64 | 22 |
39,27 | |
3 |
71,11 | 13 |
38,31 | 23 |
10,22 | |
4 |
53,41 | 14 |
39,70 | 24 |
14,63 | |
5 |
38,12 | 15 |
32,38 | 25 |
18,17 | |
6 |
41,53 | 16 |
36,12 | 26 |
20,18 | |
7 |
17,92 | 17 |
30,01 | 27 |
18,68 | |
8 |
53,00 | 18 |
42,88 | 28 |
32,13 | |
9 |
37,05 | 19 |
35,36 | 29 |
35,02 | |
10 |
60,25 | 20 |
28,16 | 30 |
31,86 |
Resonance Magnetic in Chemistry, 38(11), 977-980,2000.
